IGCSE · Chemistry 0620 · Experimental techniques & analysis

Experimental design: IGCSE Chemistry questions with answers

Free Experimental design questions for IGCSE Chemistry (0620), part of Experimental techniques & analysis. Each question has the answer and the marking points an examiner would look for.

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Experimental design practice questions

Question 1Multiple choice · 1 markA* challenge

A student needs to measure exactly 25.0 cm³ of an acid, add a varying volume of alkali from a scale, and collect the gas produced.
Which apparatus is used for each?

25.0 cm³ of acidvarying volume of alkalicollect gas
Avolumetric pipettemeasuring cylinderbeaker
Bvolumetric pipetteburettegas syringe
Cburettevolumetric pipettegas syringe
Dmeasuring cylinderburettebalance
Show answer

Answer: B

Question 2Multiple choice · 1 mark

What is the best apparatus to measure the temperature change of a reaction?

  1. A thermometer
  2. B balance
  3. C stopwatch
  4. D burette
Show answer

Answer: A

Question 3Multiple choice · 1 mark

Which statement describes solute?

  1. A A substance that is dissolved in a solvent
  2. B The Group VII elements, diatomic non-metals whose reactivity decreases down the group
  3. C The gain of oxygen, loss of electrons or increase in oxidation number
  4. D A substance that dissolves a solute
Show answer

Answer: A

Question 4Structured · 2 marks

Identify suitable apparatus for accurate measurement.

(a)

State which apparatus measures 25.0 cm³ of a solution most accurately: beaker, measuring cylinder or volumetric pipette.

[1]
(b)

Explain why a burette is used in a titration rather than a measuring cylinder.

[1]
Show answers and mark scheme
PartAnswer and marking pointsMarks
(a)volumetric pipette
volumetric pipette B1
1
(b)can add small, measured amounts accurately
measures variable volumes accurately to 0.05 cm³ / can add drop by drop B1
1
Question 5Structured · 3 marks

A student wants to find the melting point of a solid.

(a)

Suggest suitable apparatus.

[2]
(b)

State how the melting point shows if the solid is pure.

[1]
Show answers and mark scheme
PartAnswer and marking pointsMarks
(a)capillary tube, thermometer, water/oil bath
capillary tube with sample B1
thermometer in a heated water/oil bath B1
2
(b)sharp, fixed melting point
a pure substance melts at a sharp, fixed temperature (impurities lower it/give a range) B1
1
Question 6Structured · 12 marks

This question is about choosing apparatus and methods.

(a)

Name the most suitable apparatus to measure each of: exactly 25.0 cm³ of a solution; a volume of gas; the time for a reaction.

[3]
(b)

A student measures 10 cm³ of acid with a 100 cm³ measuring cylinder. Explain why this is not accurate and suggest a better choice.

[2]
(c)

Describe how to measure the rate of the reaction between magnesium ribbon and hydrochloric acid by measuring gas volume.

[4]
(d)

Explain why the student should repeat each experiment.

[1]
(e)

A gas is collected over water. Suggest a gas for which this method is unsuitable, and explain.

[2]
Show answers and mark scheme
PartAnswer and marking pointsMarks
(a)volumetric pipette; gas syringe; stopwatch
(volumetric) pipette B1
gas syringe B1
stopwatch / timer B1
3
(b)large scale divisions, large percentage error; use 10 cm³ measuring cylinder / pipette / burette
each division is large compared with 10 cm³ so the percentage error is large B1
use a 10 cm³ measuring cylinder / burette / pipette B1
2
(c)gas syringe connected to flask; add Mg, start timer; record volume at intervals; same mass/length of Mg and volume of acid
connect a conical flask to a gas syringe with a bung and delivery tube B1
add the magnesium, replace the bung and start the timer B1
record the volume of gas at regular time intervals B1
control variables: same length of magnesium, same volume and concentration of acid, same temperature B1
4
(d)to check the results are repeatable / identify anomalies
to identify anomalous results and calculate a mean (check repeatability) B1
1
(e)ammonia / hydrogen chloride; very soluble in water
ammonia / hydrogen chloride / sulfur dioxide B1
it is very soluble in water B1
2

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Original Cambridge-style practice questions written for mentorriyaz.in. These are not Cambridge past paper questions, and this site is not affiliated with or endorsed by Cambridge University Press & Assessment. Updated 2026-11-04. Paper generator · mentorriyaz.in