Experimental design: IGCSE Chemistry questions with answers
Free Experimental design questions for IGCSE Chemistry (0620), part of Experimental techniques & analysis. Each question has the answer and the marking points an examiner would look for.
A student needs to measure exactly 25.0 cm³ of an acid, add a varying volume of alkali from a scale, and collect the gas produced. Which apparatus is used for each?
25.0 cm³ of acid
varying volume of alkali
collect gas
A
volumetric pipette
measuring cylinder
beaker
B
volumetric pipette
burette
gas syringe
C
burette
volumetric pipette
gas syringe
D
measuring cylinder
burette
balance
Show answer
Answer: B
Question 2Multiple choice · 1 mark
What is the best apparatus to measure the temperature change of a reaction?
A thermometer
B balance
C stopwatch
D burette
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Answer: A
Question 3Multiple choice · 1 mark
Which statement describes solute?
A A substance that is dissolved in a solvent
B The Group VII elements, diatomic non-metals whose reactivity decreases down the group
C The gain of oxygen, loss of electrons or increase in oxidation number
D A substance that dissolves a solute
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Answer: A
Question 4Structured · 2 marks
Identify suitable apparatus for accurate measurement.
(a)
State which apparatus measures 25.0 cm³ of a solution most accurately: beaker, measuring cylinder or volumetric pipette.
[1]
(b)
Explain why a burette is used in a titration rather than a measuring cylinder.
[1]
Show answers and mark scheme
Part
Answer and marking points
Marks
(a)
volumetric pipette
volumetric pipette B1
1
(b)
can add small, measured amounts accurately
measures variable volumes accurately to 0.05 cm³ / can add drop by drop B1
1
Question 5Structured · 3 marks
A student wants to find the melting point of a solid.
(a)
Suggest suitable apparatus.
[2]
(b)
State how the melting point shows if the solid is pure.
[1]
Show answers and mark scheme
Part
Answer and marking points
Marks
(a)
capillary tube, thermometer, water/oil bath
capillary tube with sample B1 thermometer in a heated water/oil bath B1
2
(b)
sharp, fixed melting point
a pure substance melts at a sharp, fixed temperature (impurities lower it/give a range) B1
1
Question 6Structured · 12 marks
This question is about choosing apparatus and methods.
(a)
Name the most suitable apparatus to measure each of: exactly 25.0 cm³ of a solution; a volume of gas; the time for a reaction.
[3]
(b)
A student measures 10 cm³ of acid with a 100 cm³ measuring cylinder. Explain why this is not accurate and suggest a better choice.
[2]
(c)
Describe how to measure the rate of the reaction between magnesium ribbon and hydrochloric acid by measuring gas volume.
[4]
(d)
Explain why the student should repeat each experiment.
[1]
(e)
A gas is collected over water. Suggest a gas for which this method is unsuitable, and explain.
[2]
Show answers and mark scheme
Part
Answer and marking points
Marks
(a)
volumetric pipette; gas syringe; stopwatch
(volumetric) pipette B1 gas syringe B1 stopwatch / timer B1
3
(b)
large scale divisions, large percentage error; use 10 cm³ measuring cylinder / pipette / burette
each division is large compared with 10 cm³ so the percentage error is large B1 use a 10 cm³ measuring cylinder / burette / pipette B1
2
(c)
gas syringe connected to flask; add Mg, start timer; record volume at intervals; same mass/length of Mg and volume of acid
connect a conical flask to a gas syringe with a bung and delivery tube B1 add the magnesium, replace the bung and start the timer B1 record the volume of gas at regular time intervals B1 control variables: same length of magnesium, same volume and concentration of acid, same temperature B1
4
(d)
to check the results are repeatable / identify anomalies
to identify anomalous results and calculate a mean (check repeatability) B1
1
(e)
ammonia / hydrogen chloride; very soluble in water
ammonia / hydrogen chloride / sulfur dioxide B1 it is very soluble in water B1
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Original Cambridge-style practice questions written for mentorriyaz.in. These are not Cambridge past paper questions, and this site is not affiliated with or endorsed by Cambridge University Press & Assessment. Updated 2026-11-04. Paper generator · mentorriyaz.in